N CRL_PROTON
|
1H (proton)
|
16 → -4
|
16
|
1:32
|
|
N CRL_PROTON_WIDE
|
1H (wide SW)
|
30 → -10
|
16
|
1:32
|
|
N CRL_PROTON_QUANT
|
1H (quantitative)
|
16 → -4
|
4
|
2:26
|
|
N CRL_PROTON_ESPE
|
1H (solvent suppression using the excitation sculpting with perfect echo)
|
12 → -3
|
8
|
1:26
|
|
N CRL_FLUORINE
|
19F (1H coupled)
|
0 → -250
|
16
|
0:48
|
|
N CRL_FLUORINE_HDEC
|
19F (1H decoupled)
|
0 → -250
|
16
|
0:48
|
|
N CRL_FLUORINE_QUANT
|
19F (1H coupled, quantitative)
|
0 → -250
|
4
|
2:02
|
|
N CRL_FLUORINE_QUANT_HDEC
|
19F (1H decoupled, quantitative)
|
0 → -250
|
4
|
2:02
|
|
n CRL_FLUORINE_LONG
|
19F (1H coupled, long)
|
0 → -250
|
256
|
11:40
|
Yes
|
N CRL_PHOSPHORUS
|
31P (1H coupled)
|
0 → -250
|
16
|
0:54
|
|
N CRL_PHOSPHORUS_HDEC
|
31P (1H decoupled)
|
100 → -100
|
16
|
0:54
|
|
CRL_PHOSPHORUS_QUANT
|
31P (1H coupled, quantitative)
|
100 → -100
|
4
|
2:04
|
|
CRL_PHOSPHORUS_QUANT_HDEC
|
31P (1H decoupled, quantitative)
|
100 → -100
|
4
|
2:04
|
|
n CRL_PHOSPHORUS_LONG
|
31P (1H coupled, long)
|
100 → -100
|
256
|
13:01
|
Yes
|
n CRL_CARBON
|
13C (1H decoupled)
|
225 → -25
|
256
|
14:33
|
Yes
|
n CRL_CARBON_DEPTQ
|
13C DEPTQ (1H decoupled, CH/CH3 positive, C/CH2 negative)
|
225 → -25
|
256
|
14:44
|
Yes
|
n CRL_COSY
|
1H-1H COSY
|
11 → -1
|
1
|
5:07
|
Yes
|
n CRL_HSQCED
|
1H-13C HSQC (multiplicity edited)
|
1H: 11 → -1
13C: 182 → -2
|
2
|
10:02
|
Yes
|
n CRL_HMBC
|
1H-13C HMBC
|
1H: 15 → -5
13C: 224 → -45
|
2
|
31:55
|
Yes
|
n CRL_NOESY
|
1H-1H NOESY
|
11 → -1
|
4
|
24:00
|
Yes
|
